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Diazepam 10 mg. sol. iny clot, 0.5 ml. The solvent is removed and aqueous hydrochloric acid is added dropwise at room temperature to a volume of about 30 ml. The precipitate is filtered through a pad of Celite. Then the filtrate is washed with a solution of 1 M hydrochloric acid (3 or 3.5 M) in about 800 ml of ice-cold methanol. The washed filtrate is then extracted with benzene. The organic layer is washed with saturated NaHCO3 solution and dried over anhydrous sodium sulfate. The organic layer is extracted with dichloromethane to give the title compound (66 mg, 2.2 mmol). 1H-NMR (CDCl 3, 400 MHz) δ7.23 (d, J= 6.7 Hz, 1 H), 7.08 (d, J=1.9 Hz, 1 H), 2.85 (s, 3H), 1.46 (br. s, 1 H), 0.87 (t, J=8.2 Hz, 3 H). Anal. Calcd. for C 8 H 10 ClNOS: C, 68.42 H, 8.32; N, 4.88. Found: C, 68.23; H, 8.26; N, 4.81. Example 35 2,4-Dihydro-3-hydroxypyridinium 1H-NMR (CDCl 3, 500 MHz) δ 7.31 (dd, J= 8.0, 0.2 Hz, 2 H), 7.32-7.35 (dd, J=8.1, 0.2 Hz, 2 H), 3.84-4.16 (m, 4 2.97-3.01 2 H), 1.54-1.80 (t, J=7.3 Hz, 3 H). Found: C, 65.20 H, 8.38; N, 4.66. Example 36 A mixture of 2,2'-Di-5-hydroxybutyrate and 2,4-dihydro-1-hydroxypyridinium, stirred at room temperature for 24 hours. The reaction mixture was extracted with EtOAc/HCl (5%), then dried over anhydrous sodium sulfate. The residue was purified by flash chromatography eluting with hexane-ethyl acetate:EtOAc (2:1) to give 2,4-dihydro-3-hydroxypyridinium as a clear oil. ESI-MS (mass resolution 1.43 mol. %) was used for analysis. Example 37 The 4-hydroxy, 5,4'-dihydroxy-5-methyl-2-hydroxypyridine (methoxy) (6a) is prepared by the addition of 4-hydroxy, 5,4'-di(2-methylbutyl)methanone (50g) in CH 2 Cl (10.0 ml). The reaction mixture is slowly heated to 70° C. and quenched with saturated NaOH solution (1.0 M, 10 mL) and water. The mixture is stirred for 2 hours and a solution of methoxy ester is added, stirring for 5 minutes. The resulting oil is filtered through a Pad of Celite and then washed with 1 M concentrated HCl solution. The crude mixture was dissolved into Et 2 O (1 :1) cheap kamagra for sale uk and extracted with Et 2 O (2 × min. ) to give a clear oil. The water-free, eluted product was purified by flash chromatography eluting with hexane-ethyl acetate:EtOAc (2:1) to give the subtitle compound (2,4-Dihydro-5-methyl-2-hydroxypyridinium): 0.9 mmol. (39 mg). Example 38 The 4-hydroxy, 5,4'-dihydroxy-5-methyl-2-hydroxypyridine (methoxy) (6b) is prepared by the addition of 4-hydroxy, 5,4'-di(2-methylbutyl)methanone (50g) and sodium hydroxide (10 M) in CH 2 Cl (1.0 M, 10 mL) and water to give 5-methyl-4-hydroxy-2-methylbutylpyridine in 7.2 ml of CH 2 Cl (3 × 5 min.). The procedure is followed until a water-free oil is obtained. The crude material was dissolved in Et 2 O (3 :1) and extracts were.

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